Bragg’s Law: Plane Spacing d

Known X-ray λ. For orders n = 1, 2, 3 find the grazing angle of the intensity peak and recover d from a fit of sin θ versus n.

University / research· 24 min·Related simulator: Optics & LightBragg’s Law (X-ray)

Goal

Determine d from 2 d sin θ = n λ. A plot of sin θ versus n has slope λ/(2d), so d = λ / (2 · slope).

Equipment

  • X-ray line (known λ)
  • Unknown crystal
  • Goniometer
  • Intensity detector

Experiment

Theory

Constructive interference from crystal planes obeys Bragg’s law. The bench hides d, 2d sin θ and any “match” flag. λ is known (Cu Kα). A live detector intensity is the instrument — you hunt the peak for each order.

Procedure

  1. Wavelength λ is fixed and known. d is hidden. Set the order n, then sweep the grazing angle θ.
  2. Watch the live detector. Park at the intensity peak. The bench does not print “Bragg matched”.
  3. Record. The row stores n and θ. The notebook computes sin θ.
  4. Repeat for n = 1, 2 and 3 (two records per order is fine). At least 6 rows.
  5. Fit sin θ versus n; d = λ / (2 · slope). Compare with the reference.

Conclusion

The fitted d agrees with the hidden plane spacing. Main uncertainties: goniometer steps and judging the intensity peak by eye.