Bragg’s Law: Plane Spacing d
Known X-ray λ. For orders n = 1, 2, 3 find the grazing angle of the intensity peak and recover d from a fit of sin θ versus n.
Goal
Determine d from 2 d sin θ = n λ. A plot of sin θ versus n has slope λ/(2d), so d = λ / (2 · slope).
Equipment
- X-ray line (known λ)
- Unknown crystal
- Goniometer
- Intensity detector
Experiment
Theory
Constructive interference from crystal planes obeys Bragg’s law. The bench hides d, 2d sin θ and any “match” flag. λ is known (Cu Kα). A live detector intensity is the instrument — you hunt the peak for each order.
Procedure
- Wavelength λ is fixed and known. d is hidden. Set the order n, then sweep the grazing angle θ.
- Watch the live detector. Park at the intensity peak. The bench does not print “Bragg matched”.
- Record. The row stores n and θ. The notebook computes sin θ.
- Repeat for n = 1, 2 and 3 (two records per order is fine). At least 6 rows.
- Fit sin θ versus n; d = λ / (2 · slope). Compare with the reference.
Conclusion
The fitted d agrees with the hidden plane spacing. Main uncertainties: goniometer steps and judging the intensity peak by eye.